標題: Analysis of prostaglandins by micellar electrokinetic capillary chromatography
作者: Hsieh, YZ
Kuo, KL
交大名義發表
應用化學系
National Chiao Tung University
Department of Applied Chemistry
關鍵字: buffer composition;prostaglandins;thromboxanes
公開日期: 14-二月-1997
摘要: This paper presents a rapid and reliable micellar electrokinetic capillary chromatography (MEKC) method to separate major prostaglandins and thromboxane B-2. The running buffer was modified with sodium dodecyl sulfate (SDS). The effects of the SDS concentration on the migration behavior of analytes was also examined. Moreover, the influences of electrolyte concentration and capillary temperature on the separation were investigated. In optimum conditions, seven major prostaglandins and thromboxane B-2 could be separated within 8 min. The relative standard deviations of the migration times (reproducibility) of the analytes were less than 0.82%.
URI: http://dx.doi.org/10.1016/S0021-9673(96)00795-9
http://hdl.handle.net/11536/724
ISSN: 0021-9673
DOI: 10.1016/S0021-9673(96)00795-9
期刊: JOURNAL OF CHROMATOGRAPHY A
Volume: 761
Issue: 1-2
起始頁: 277
結束頁: 284
顯示於類別:期刊論文


文件中的檔案:

  1. A1997WM84600027.pdf