標題: Synthesis and characterization of semicarbazone of p-hydroxy-3-methoxy acetophenone (SPH3MA) single crystal
作者: Janarthanan, S.
Rajan, Y. C.
Umarani, P. R.
Selvakumar, S.
Pandi, S.
材料科學與工程學系
Department of Materials Science and Engineering
關鍵字: Solution crystal growth;Organic compounds;UV absorption;X-ray diffraction
公開日期: 15-一月-2011
摘要: Single crystals of semicarbazone of p-hydroxy-3-methoxy acetophenone (SPH3MA) were grown by a slow evaporation solution growth technique at room temperature. This is the first report in the literature on the crystallization of SPH3MA. The cell parameters of the grown crystals were estimated by single crystal X-ray diffraction analysis. The various planes of reflection were identified from the XRD powder pattern. The presence of functional groups was identified from FTIR and (1)H NMR. The results were found to be in accordance with the structure of the crystal. The formation of charge transfer complex was confirmed by UV-vis-NIR spectroscopy. The thermal stability of the grown crystal was studied by thermal analysis. (C) 2010 Elsevier B.V. All rights reserved.
URI: http://dx.doi.org/10.1016/j.physb.2010.09.010
http://hdl.handle.net/11536/25877
ISSN: 0921-4526
DOI: 10.1016/j.physb.2010.09.010
期刊: PHYSICA B-CONDENSED MATTER
Volume: 406
Issue: 2
起始頁: 135
結束頁: 138
顯示於類別:期刊論文


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